Synthesis of TiO2 nanoparticles in pure 2-hydroxyethylammonium formate room temperature ionic liquid and investigation of its photocatalytic properties

Authors

  • Fatemeh Fallah Iri Sola -
  • Mohammad Khodadadi Moghaddam -
Abstract:

TiO2 nanoparticles were synthesized by modified sol—gel method using pure room temperature ionic liquid(RTIL) 2-hydroxyethylammonium formate as a reaction medium. The structure and morphology of TiO2nanoparticles were characterized with X-ray powder diffraction (XRD), BET surface analysis and scanningelectron microscopy (SEM). TiO2 nanoparticles were synthesized in open and closed vessels. The TiO2nanoparticles prepared in open vessel present only anatase crystal phase after calcination at 500°C but the TiO2prepared in closed vessel presents anatase and rutile phases after calcination at 500°C. The photocatalyticefficiency decreases with increasing of ethanol and water as molecular solvent in preparation step ofnanoparticles. The degradation percent can reach over 97% at the optimal catalyst concentration (2.0 g/L) in 120minutes irradiation.

Upgrade to premium to download articles

Sign up to access the full text

Already have an account?login

similar resources

synthesis of tio2 nanoparticles in pure 2-hydroxyethylammonium formate room temperature ionic liquid and investigation of its photocatalytic properties

tio2 nanoparticles were synthesized by modified sol—gel method using pure room temperature ionic liquid(rtil) 2-hydroxyethylammonium formate as a reaction medium. the structure and morphology of tio2nanoparticles were characterized with x-ray powder diffraction (xrd), bet surface analysis and scanningelectron microscopy (sem). tio2 nanoparticles were synthesized in open and closed vessels. the ...

full text

synthesis of 3-aryl-2h-benzo[b]-1,4-oxazines in [omim]bf4 and reduction of organic compounds in methylimidazolium formate

در این پروژه ترکیبات 3-آریل-2h-بنزو[b]-4،1-اکسازین ها از مواد اولیه تجاری مشتقات دو آمینو فنول و ?-هالو کتون های آروماتیک در مایع یونی 1-اکتیل-3-متیل ایمیدازولیوم تترا فلورو بورات([omim]bf4) سنتز شده است. این واکنش توسط باز پتاسیم کربنات محلول از طریق o-آلکیلاسیون و سپس یک واکنش آمیداسیون درون مولکولی خود بخود در مدت زمان کوتاه انجام می شود. ترکیبات 4،1-بنزوکسازین به این روش با بهره خوب تا آلی ...

15 صفحه اول

control of the optical properties of nanoparticles by laser fields

در این پایان نامه، درهمتنیدگی بین یک سیستم نقطه کوانتومی دوگانه(مولکول نقطه کوانتومی) و میدان مورد مطالعه قرار گرفته است. از آنتروپی ون نیومن به عنوان ابزاری برای بررسی درهمتنیدگی بین اتم و میدان استفاده شده و تاثیر پارامترهای مختلف، نظیر تونل زنی(که توسط تغییر ولتاژ ایجاد می شود)، شدت میدان و نسبت دو گسیل خودبخودی بر رفتار درجه درهمتنیدگی سیستم بررسی شده اشت.با تغییر هر یک از این پارامترها، در...

15 صفحه اول

Synthesis of mesoporous TiO2-SiO2-Ag and investigation of its structural and photocatalytic properties under visible light and ultra-violate

In this project, mesoporous titanium oxide-silicon oxide doped by silver (TiO2-SiO2-Ag) was hydrothermally synthesized. Titanium isopropoxide, tetraethyl orthosilicate and silver nitrate were used as precursors for TiO2, SiO2 and Ag, respectively. Initially TiO2-SiO2 mesoporous nanocomposite was synthesized with weight ratios of silica to titania SiO2:TiO2:3:1 via hydrothermal method at 70˚C an...

full text

Ionic liquid-assisted synthesis, characterization and photocatalytic properties of SnO microflowers with nanosheet subunits

In this study, simple ionic liquid-assisted preparation of SnO microflowers with nanosheet subunitsunder reflux condition without calcination were described. Samples were synthesized using 1-pentyl-3-methylimidazolium bromide, [pmim]Br, as an ionic liquid in different molar ratio, sodium hydroxideand Tin(II) chloride. The results show that SnO with high purity and uniform size...

full text

My Resources

Save resource for easier access later

Save to my library Already added to my library

{@ msg_add @}


Journal title

volume 7  issue 4

pages  37- 44

publication date 2011-02-01

By following a journal you will be notified via email when a new issue of this journal is published.

Hosted on Doprax cloud platform doprax.com

copyright © 2015-2023